Heating Actinide Materials in a 2.9 volume % Hydrogen Atmosphere Using a Laboratory Furnace in the C-155 Glovebox
CX(s) Applied: B3.6
Location(s): South Carolina
Offices(s): Savannah River Operations Office
The preparation of uranium (IV) oxide (UO2) and mixed actinide oxides containing UO2 can be accomplished by heating actinide compounds in the presence of hydrogen. Hydrogen is required as a reducing agent to prevent the oxidation of U(IV) to a higher oxidation state. The capability to heat actinide materials in a reducing environment using 2.9 volume % hydrogen in Ar was installed in glovebox 46 in lab C-155. Multiple research and demonstration programs will utilize the furnace capability to prepare actinide oxides.